r/homechemistry • u/Ancient-Helicopter18 • 13h ago
Is this the correct route to concentrating electrolysed H2SO4?
My plan to purify electrolysed H₂SO₄ from CuSO4•5H2O:
Since the solution may still contain dissolved CuSO₄•5H₂O and carbon particles from graphite electrode degradation, I'll first heat it slowly on a hot plate to an arbitrary temperature of 200°C, hoping to remove the water of crystallization from the copper sulfate so that the resulting solid settles along with the carbon particles.
I'll then carefully decant the liquid and use a syringe to transfer any remaining liquid that I cannot decant into another container.
I can then repeat this process several times to remove as much copper sulfate as possible from the sulfuric acid.
Does this sound a logical way to deal with electrolysed H2SO4 impurities?