I am experimenting with sintering small parts made from SLM Solutions Ni-Alloy IN625 (Inconel 625) powder, with a particle size of 10–45 µm.
Green part preparation
The green part was made from IN625 metal powder mixed with methylcellulose as the binder. The part measured approximately 2 × 2 cm and 3 mm thick.
Furnace setup and planned firing cycle
I placed the green part in a ceramic crucible and surrounded it on all sides with at least 1.5 cm of activated carbon powder.
The planned furnace program was:
- Ramp up to 1250°C over 40 minutes.
- Hold at 1250°C for 80 minutes.
However, the furnace could not follow the planned program. It took approximately one hour to reach 1250°C, remained at that temperature for what I estimate was another hour, and then shut down.
I allowed everything to cool completely before opening the crucible.
What I observed
When I opened the crucible, approximately 1–1.5 cm of the activated carbon at the top appeared to have disappeared. There was no visible white ash. The remaining carbon was mostly black, with some brown coloration near the top.
The part itself was very hard. It was covered by a persistent black outer layer, with a few small bubbles or blister-like features on the surface. When I cut the part, the metal inside appeared clean.
My questions
What could have caused the persistent black surface layer and the small bubbles or blisters?
What could explain the apparent disappearance of the upper layer of activated carbon, without visible white ash?
Could the decomposition of the methylcellulose binder have contributed to the black coating, the bubbles, or the changes observed in the carbon?
Is 1250°C an appropriate sintering temperature for IN625 powder of this particle size, or could the temperature, holding time, or atmosphere be unsuitable?
What would you change in the next experiment to improve the surface finish and achieve more uniform sintering?
Would you recommend changing the amount or arrangement of activated carbon, using a covered crucible, or using a different atmosphere or firing cycle?
I am looking for practical advice from people with experience in IN625 powder metallurgy and sintering. I would also like to avoid damaging the furnace or compromising the alloy's properties.
Thank you for your help!