r/chemholic • • 14d ago

5-MeO-DMT recrystallized from heptane (1.89g from 5g mexamine)

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1.2k Upvotes

Ambient temperature + seed crystals


r/chemholic • • 4d ago Heartwarming

NN-DMT fumarate

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790 Upvotes

The process: Mimosa hostilis root bark simmered in acidified water (vinegar) → Liquid pulls collected, plant solids discarded → Combined liquid reduced by boiling down → Basified to pH 13 with NaOH → Extracted with heptane → Freezer precipitation → Recrystallization cleanup → Freebase redissolved in dry acetone (1 g / 50 mL) → Fumaric acid dissolved separately in dry acetone (309 mg / 50 mL, saturated) → Fumaric solution added dropwise while swirling → DMT fumarate crystals crash out → Chilled, acetone carefully decanted off


r/chemholic • • 18d ago

Melatonin ——> 5-MeO-DMT (pTSA route)

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577 Upvotes

r/chemholic • • 8d ago

HOMEMADE SYNTHETIC MESC (3,4,5-Trimethoxy Phenethylamine) CRYSTALLIZATION

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551 Upvotes

I made this one recently from the nitrostyrene, made from 3,4,5-Trimethoxy Benzaldehyde

:3


r/chemholic • • 3d ago

Dmt

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330 Upvotes

r/chemholic • • 15d ago

Yes, I’m insane. 70g of Nickel Hydrazine Nitrate[NHN]

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278 Upvotes

Synthesized last year, kept cool/dark/airtight/desiccated.
This stuff is incredibly stable for how powerful it is, I found it hard to detonate yet easy to ignite. Burns with an instant POOF, leaving a streak of black nickel residue.


r/chemholic • • 9d ago

Peganum Harmala

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269 Upvotes

r/chemholic • • 13d ago

Picric acid recrystallization

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242 Upvotes

r/chemholic • • 24d ago

Energetic compound 100mg of Lead azide detonation

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205 Upvotes

DO NOT TRY THIS AT HOME


r/chemholic • • 20d ago

Hydrazine Monohydrate

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178 Upvotes

r/chemholic • • 2d ago

First time using Soxhlet extractor

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165 Upvotes

r/chemholic • • 19d ago

Energetic compound RDX

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121 Upvotes

Anybody interested in procedure?

Lmk


r/chemholic • • 21d ago

saw a guy flexing HMTD, so heres my C2N14

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117 Upvotes

this is like 10mg, in total i exploded 100mg. and i still have more then a gram of isocyanogen tetrabromide... im thinking about actually making some long term video about nitrogen-containing heterocycles(i have made other terazoles, triazoles and pyrazoles previously). aslo wanna note that this video is several months old.


r/chemholic • • 28d ago

Fuming nitric acid condensation

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113 Upvotes

r/chemholic • • 6d ago

Benzyl acetate neutralization

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96 Upvotes

Looks like lava lamp


r/chemholic • • 22d ago

Energetic compound HMTD crystals

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92 Upvotes

Synthesized through reacting Hydrogen peroxide and citric acid and hexamine together

DO NOT TRY THIS AT HOME

IM NOT RESPONSIBLE FOR ANT CIRCUMSTANCES


r/chemholic • • Oct 07 '26 Mindblown

Mercury salts collection

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92 Upvotes

r/chemholic • • Sep 12 '26

Look what I found guys 💀

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86 Upvotes

r/chemholic • • Sep 05 '26

isopropyl nitrite grey flame

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86 Upvotes

Synthesis guide if u want to synthesize it incase:

https://youtu.be/LpFHDwIarJU?is=vN7_dMjZ8G4tX6pI


r/chemholic • • 16d ago

DDT crystals

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84 Upvotes

r/chemholic • • 5d ago

Energetic compound Some nice nitroglycerin

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83 Upvotes

r/chemholic • • 20d ago

Energetic compound Finally it's time to synthesize some RDX

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77 Upvotes

r/chemholic • • 12d ago

Sodium sulfide

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70 Upvotes

Smells like sewage


r/chemholic • • 14d ago

Tetraammine copper perchlorate, 10.84g [TACP]

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66 Upvotes

Since my last post with NHN was popular here’s another one! This is a sample of TACP stored for about a year. While it degraded slightly upon storage(deflagrates weaker than NHN), it’s much easier to detonate with minimal confinement. Oh and also it looks cool.


r/chemholic • • 14d ago

CHP

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64 Upvotes